14. marts 2017

Lynhurtig kvalitetskontrol på foder

Kvalitetskontrol af råvarer, ingredienser, mix eller færdigvarer med Røntgen Flourescens er nu hurtigere og bedre end nogensinde.

Kvalitetskontrol af råvarer, ingredienser, mix eller færdigvarer med Røntgen Flourescens er nu hurtigere og bedre end nogensinde.

Bestemmelse af Na, Mg, P, Cl, K, Ca, Mn, Fe og mange flere, med detektions grænser fra 1 ppm - måles direkte, uden nævneværdig prøve forberedelse.

Takket være den rivende udvikling af detektorer, optik og med Rigaku's RFP-SQX software, måles alle elementer på én gang og uden kalibrering.

Læs hele "Analysis of Animal Feeds"-applikationen fra Rigaku her. 

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10. februar 2017

Stony-iron meteorite analysis

Analysis of a stony-iron meteorite using a HyPix-3000 multi-dimensional detector.

Introduction
A stony-iron meteorite is like a single crystal. When using 0- or 1-dimensional detectors, only a few diffraction peaks are observed. In this situation, identification of crystalline phases cannot be conducted. Therefore, a stony-iron meteorite was analyzed using the multi-dimensional detector, HyPix-3000, which has an effective detection area for the identification of crystalline phases.

 

 

Measurements and results
A stony-iron meteorite was analyzed using the HyPix-3000. Inside a stony-iron meteorite, there are transparent parts similar to glass and opaque parts similar to metal. The transparent parts were thought to be non-crystalline (amorphous). However, when measurement of the transparent part was actually performed, only one diffraction line was observed. In general, when measurement is done with a 0D or a 1D detector, the range in which diffraction X-rays can be detected from the sample is limited to a certain region. (This region is indicated in yellow in Fig. 1.) In this experiment, the diffraction lines, indicated with red arrows, are within the scanning range, and therefore can be detected. On the other hand, it is possible to acquire information on multiple lattice planes, as shown in Fig. 2, by using the HyPix-3000, which has a wide effective detection area, and by performing measurement while oscillation the sample. When the 2D diffraction image obtained in Fig. 2 was converted to a 2θ-I profile and qualitative analysis of the transparent part was carried out, it was possible to identify forsterite (Mg₂SiO₄) (Fig. 3). Since diffraction spots were observed, it was conjectured that the glass-like transparent part is a single crystal or is comprised of an extremely small number of crystal grains.

 

 

 

 

 

 

Fig. 1: X-ray diffraction pattern of glass-like transparent part when using a 0D or 1D detector

 

 

 

 

 

 

 

 

 

 

 

 

 

 

 

Fig. 2: 2D diffraction image of transparent part (with oscillation)

 


Fig. 3: Result of qualitative analysis of transparent part


Recommended equipment and software

  • Automated Multipurpose X-ray Diffractometer SmartLab
  • 2D Hybrid Pixel Array Detector HyPix-3000

 

 

 

 

 

 

 

 

 

The SmartLab is the most novel high-resolution diffractometer available today.  
Perhaps its most novel feature is the SmartLab Guidance software,
which provides the user with an intelligent interface that guides you through the intricacies of each experiment. It is like having an expert standing by your side.
For more information click here.

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